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Nuclear Magnetic Resonance(NMR)

Nuclear Magnetic Resonance(NMR)

Nuclear Magnetic Resonance(NMR)

Make: Bruker

Model: AVANCE III HD, Ascend TM WB, 500 MHz

Capabilities

Specifications

  • Frequency: 500 MHz
  • Magnetic Field: 11.7 Tesla
Probes/Accessories available:
1. BBFO Probe (Liquid State): Broad Band Fluorine observe
  • Inner coil optimized for observation of nuclei between 31P and 15N (BBFO: for 19F as well)
  • Sample diameter: 5 mm (BBFO)
  • Switch between decoupling nuclei using an automated tuning and matching device (ATM).
  • Z-Gradient at all frequencies
  • Variable Temperature range from +150 to -150
  • Maximum gradient strength is 50 gauss/cm
2. TBI Probe (Liquid State):
  • A 5mm Inverse Triple-resonance probe-head in multinuclear version,
  • TBI (1H, 31P, BB) with Z-gradient.
  • The BB range is 109Ag-31P.
  • Variable Temperature range from +150 to -150
3. Diffusion Probe: 1H(offers 3D gradients)

Types of Experiment can be conducted: 1D NMR, DEPT, 2D NMR: COSY, TCOSY, DOSY, NOESY, ROESY, HMQC, HSQC, Water Suppression Experiment, Multinuclear NMR, Variable temperature measurement
Sample Requirement: 5 mg for 1H and minimum 10 mg for 13C NMR experiment. Compounds should be highly pure and soluble in 0.6 ml Deuterated solvent.


Application:

  • Materials characterization can be done using NMR Diffusion and relaxation experiments.
  • Structural elucidation of organic, inorganic, and organometallic compounds; purity testing and compound identification.
  • Analysis of binding interactions, kinetics, and conformational changes in drug discovery and molecular recognition.

Sample Requirement

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Charges

Academics(Rs)+18% GST Industry(Rs)+18% GST
 Proton: 500/Sample
Low X Nuclei: 1000/Sample/1hr
High X Nuclei: 500/Sample
2D NMR: 500/Sample
Solid 1D (1H/X): 2000/Sample
Solid 2D (X): 5000/Sample
Proton: 500/Sample
low X Nuclei: 1000/Sample/1hr
High X Nuclei: 500/Sample
2D NMR: 1500/Sample
Solid 1D (1H/X): 5000/Sample
Solid 2D (X): 8000/Sample

Publications

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Contact Us

Name: Dr Jayita Sarkar

Designation: Snr Scientific Officer

Phone:0291 280 1343

Email:jsarkar[at]iitj[dot]ac[dot]in

Name: Dr Saloni Sharma

Designation: Scientific Officer

Phone:0291 280 1347

Email:saloni[at]iitj[dot]ac[dot]in

Name: Mr lalit Mohan

Designation: Junior Assistant

Phone:0291 280 1344

Email:

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